Record Details

Title The Ph Dependent Thermal Stability of the Organic Tracers 1,5-NDS and 2-NSA
Authors L. Sajkowski, B.W. Mountain, T.M. Seward
Year 2016
Conference New Zealand Geothermal Workshop
Keywords Tracer studies, naphthalene disulfonic acid, naphthalene sulfonic acid, NDS, NSA, experimental geochemistry.
Abstract The pH dependence of the thermal stability of 1,5-naphthalene disulfonate and 2-naphthalene sulfonate have been investigated. The experiments were conducted using batch autoclave reactors. Two experimental temperatures were investigated (200℃, 300℃). The pH ranged from 3 to 9.85 and two ionic strengths were used (0.001 M, 0.05 M). The duration of each experiment was 40 hours.
The results show that:
1) 1,5-NDS is not stable at 300°C, pH 3, 4, 9 and 9.85, I = 0.001M, 0.05M;
2) 1,5-NDS is stable at 200°C, pH 4, I=0.001 M;
3) the low thermal stability of 1,5-NDS can be explained by two mechanisms: steric hindrance and kinetics;
4) 2-NSA is stable at 200°C pH 3, 4, 9 and 9.85, I = 0.001M, 0.05M;
5) the stability of 2-NSA at 300°C is independent of ionic strength;
6) 2-NSA is thermally stable at 300°C and pH 9.85, I = 0.05 M;
Further experiments are underway to confirm and expand our knowledge
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